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Two procedures for degassing are common. The first is known as freeze-pump-thaw — the solvent is frozen under liquid nitrogen, and a vacuum is applied. Thereafter, the stopcock is closed and the solvent is thawed in warm water, allowing trapped bubbles of gas to escape. [4]
In January 2021, a line carrying liquid nitrogen ruptured at a poultry processing plant in the U.S. state of Georgia, killing six people and injuring 11 others. [19] Because of its extremely low temperature, careless handling of liquid nitrogen and any objects cooled by it may result in cold burns. In that case, special gloves should be used ...
The liquid nitrogen wash has two principle functions: [1] Removal of impurities such as carbon monoxide, argon and methane from the crude hydrogen gas; Addition of the required stoichiometric amount of nitrogen to the hydrogen stream to achieve the correct ammonia synthesis gas ratio of hydrogen to nitrogen of 3 : 1
Sanitation Standard Operating Procedures is the common name, in the United States, given to the sanitation procedures in food production plants which are required by the Food Safety and Inspection Service of the USDA and regulated by 9 CFR part 416 in conjunction with 21 CFR part 178.1010.
A standard operating procedure (SOP) is a set of step-by-step instructions compiled by an organization to help workers carry out routine operations. [1] SOPs aim to achieve efficiency, quality output, and uniformity of performance, while reducing miscommunication and failure to comply with industry regulations .
The inert-gas line is vented through an oil bubbler, while solvent vapors and gaseous reaction products are prevented from contaminating the vacuum pump by a liquid-nitrogen or dry-ice/acetone cold trap. Special stopcocks or Teflon taps allow vacuum or inert gas to be selected without the need for placing the sample on a separate line. [3]
A tank of liquid nitrogen, used to supply a cryogenic freezer (for storing laboratory samples at a temperature of about −150 °C or −238 °F) Controlled-rate and slow freezing, also known as slow programmable freezing (SPF), [18] is a technique where cells are cooled to around -196 °C over the course of several hours.
Cryogenic IQF freezers immerse the product in liquid nitrogen at very low temperatures, freezing it rapidly while continuously moving the product to avoid block or lump formation. [5] Although this method shows good freezing results, it might lead to higher processing costs per weight of product due to the cost of the liquid nitrogen required.
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