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  2. Work-up - Wikipedia

    en.wikipedia.org/wiki/Work-up

    The Grignard reaction between phenylmagnesium bromide (1) and carbon dioxide in the form of dry ice gives the conjugate base of benzoic acid (2). The desired product, benzoic acid (3), is obtained by the following work-up: [2] Synthesis of benzoic acid with work-up step in red.

  3. McMurry reaction - Wikipedia

    en.wikipedia.org/wiki/McMurry_reaction

    The McMurry reaction of benzophenone. The McMurry reaction is an organic reaction in which two ketone or aldehyde groups are coupled to form an alkene using a titanium chloride compound such as titanium(III) chloride and a reducing agent.

  4. Synthesis of nucleosides - Wikipedia

    en.wikipedia.org/wiki/Synthesis_of_nucleosides

    More than about 1.2-1.4 equivalents of Lewis acid are rarely needed. Acetonitrile is the most common solvent employed for these reactions, although other polar solvents are also common. Workup of reactions employing TMSOTf involves treatment with an ice-cold solution of sodium bicarbonate and extraction of the resulting sodium salts.

  5. Acid–base extraction - Wikipedia

    en.wikipedia.org/wiki/Acid–base_extraction

    Acid–base extraction is a subclass of liquid–liquid extractions and involves the separation of chemical species from other acidic or basic compounds. [1] It is typically performed during the work-up step following a chemical synthesis to purify crude compounds [2] and results in the product being largely free of acidic or basic impurities.

  6. Friedel–Crafts reaction - Wikipedia

    en.wikipedia.org/wiki/Friedel–Crafts_reaction

    The Friedel–Crafts reactions are a set of reactions developed by Charles Friedel and James Crafts in 1877 to attach substituents to an aromatic ring. [1] Friedel–Crafts reactions are of two main types: alkylation reactions and acylation reactions. Both proceed by electrophilic aromatic substitution. [2] [3] [4] [5]

  7. Puzzle solutions for Saturday, Nov. 30, 2024

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    This article originally appeared on USA TODAY: Online Crossword & Sudoku Puzzle Answers for 11/30/2024 - USA TODAY. Show comments. Advertisement. Advertisement. Holiday Shopping Guides.

  8. Corey–House synthesis - Wikipedia

    en.wikipedia.org/wiki/Corey–House_synthesis

    The scope of the Corey-House synthesis is exceptionally broad, and a range of lithium diorganylcuprates (R 2 CuLi, R = 1°, 2°, or 3° alkyl, aryl, or alkenyl) and organyl (pseudo)halides (RX, R = methyl, benzylic, allylic, 1°, or cyclic 2° alkyl, aryl, or alkenyl and X = Br, I, OTs, or OTf; X = Cl is marginal) will undergo coupling as the nucleophilic and electrophilic coupling partners ...

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  1. Related searches aqueous workup mechanism example answer page 5 1 6 2 through 20 even

    aqueous workup mechanism example answer page 5 1 6 2 through 20 even integer