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A melting-point apparatus is a scientific instrument used to determine the melting point of a substance. Some types of melting-point apparatuses include the Thiele tube , Fisher-Johns apparatus, Gallenkamp (Electronic) melting-point apparatus and automatic melting-point apparatus.
During heating, the point at which melting is observed and the temperature constant is the melting point of the sample. [1] A more modern method uses dedicated equipment, known as a melting point apparatus. A slow heating rate at the melting point is needed in order to get an accurate measurement.
This melting-point apparatus for use with a microscope was developed by the Austrian pharmacognosist Ludwig Kofler (30 November 1891 Dornbirn - 23 August 1951 Innsbruck) and his wife mineralogist Adelheid Kofler. In 1936, the Koflers and Mayrhofer published their "Mikroskopische Methoden in der Mikrochemie" [Kofler, L., A.
The melting point (or, rarely, ... exist for the determination of melting points. ... melting point meter. A basic melting point apparatus for the analysis of ...
Thermogravimetric analysis or thermal gravimetric analysis (TGA) is a method of thermal analysis in which the mass of a sample is measured over time as the temperature changes. . This measurement provides information about physical phenomena, such as phase transitions, absorption, adsorption and desorption; as well as chemical phenomena including chemisorptions, thermal decomposition, and ...
Thermogravimetric Analysis (TGA) may be more useful for decomposition behavior determination. Impurities in polymers can be determined by examining thermograms for anomalous peaks, and plasticisers can be detected at their characteristic boiling points. In addition, examination of minor events in first heat thermal analysis data can be useful ...
The Slip melting point (SMP) or "slip point" is one conventional definition of the melting point of a waxy solid. It is determined by casting a 10 mm column of the solid in a glass tube with an internal diameter of about 1 mm and a length of about 80 mm, and then immersing it in a temperature-controlled water bath .
The apparatus is heated. Dissolved gases evolve from the sample first, and the air in the capillary tube expands. Once the sample starts to boil, heating is stopped, and the temperature starts to fall. The temperature at which the liquid sample is sucked into the sealed capillary is the boiling point of the sample. [1] [2] [3] [4]
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