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The thermal conductivity detector (TCD), also known as a katharometer, is a bulk property detector and a chemical specific detector commonly used in gas chromatography. [1] This detector senses changes in the thermal conductivity of the column eluent and compares it to a reference flow of carrier gas. Since most compounds have a thermal ...
Thermal radiation () End losses through the support structures; A heated metal wire (sensor wire, or simply sensor) suspended in a gas will lose heat to the gas as its molecules collide with the wire and remove heat. If the gas pressure is reduced, the number of molecules present will fall proportionately and the wire will lose heat more slowly.
The transient hot wire method has advantage over the other thermal conductivity methods, since there is a fully developed theory and there is no calibration or single-point calibration. Furthermore, because of the very small measuring time (1 s) there is no convection present in the measurements and only the thermal conductivity of the fluid is ...
The range of thermophysical properties can be covered by different forms of the technique, with the exception that the recommended thermal conductivity range where the highest precision can be attained is 0.01 to 150 W/m•K for the linear source freestanding sensor and 500 to 8000 J/m2•K•s0.5 for the planar source freestanding sensor.
A pellistor is a solid-state device [1] used to detect gases which are either combustible or which have a significant difference in thermal conductivity to that of air. The word "pellistor" is a combination of pellet and resistor .
Simplified schematic of a single gap chemiresistive sensor. (not to scale) A chemiresistor is a material that changes its electrical resistance in response to changes in the nearby chemical environment. [1] Chemiresistors are a class of chemical sensors that rely on the direct chemical interaction between the sensing material and the analyte. [2]
Time-domain thermoreflectance (TDTR) is a method by which the thermal properties of a material can be measured, most importantly thermal conductivity. This method can be applied most notably to thin film materials (up to hundreds of nanometers thick), which have properties that vary greatly when compared to the same materials in bulk. The idea ...
Flow controllers are used to add hydrogen (for example, 10% hydrogen in nitrogen). The composition of the gaseous mixture is measured at the exit of the sample container with appropriate detectors (thermal conductivity detector, mass spectrometer). Now, the sample in the oven is heated up on predefined values.
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