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Septa seal the two conical flasks. A cannula is used to transfer THF from the flask on the right to the flask on the left.. Cannula transfer or cannulation is a set of air-free techniques used with a Schlenk line, in transferring liquid or solution samples between reaction vessels via cannulae, avoiding atmospheric contamination.
the use of syringes and rubber septa to transfer liquids and solutions; [6] cannula transfer, where liquids or solutions of air-sensitive reagents are transferred between different vessels stoppered with septa using a long thin tube known as a cannula. Liquid flow is supported by vacuum or inert-gas pressure.
A Schlenk flask, or Schlenk tube, is a reaction vessel typically used in air-sensitive chemistry, invented by Wilhelm Schlenk.It has a side arm fitted with a PTFE or ground glass stopcock, which allows the vessel to be evacuated or filled with gases (usually inert gases like nitrogen or argon).
The rubber bung may be used to seal a flask because the user may require the contents to be mixed via shaking the flask or may require that the contents be kept inside the flask and prevented from leaking out. In all cases, the bung keeps the experimentation environment sealed so that liquids or gases cannot escape (or enter). [citation needed]
The inner flask contains liquid helium and the outer flask contains liquid nitrogen, with one vacuum section in between. The loss of precious helium is limited in this way. Other improvements to the vacuum flask include the vapour-cooled radiation shield and the vapour-cooled neck, [11] both of which help to reduce evaporation from the flask.
It is often used in combination with a Büchner flask, Büchner ring and sinter seals. A vacuum tight seal and stability of the Büchner flask and filter are essential during the filtration process. A Büchner ring can be used with Büchner funnels, flasks, glass crucibles and Gooch crucibles. The wide flange and large surface contact ensures ...
Büchner flask A Büchner funnel is attached to the flask via a black elastomer adapter. The hose barb is connected via vacuum hose to a vacuum source such as an aspirator. The flask should be clamped before use or the hose will likely cause it to tip. Cross section of a Büchner Flask. Note the hose barb pointing right for attaching a vacuum ...
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