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A simple short path vacuum distillation apparatus can be used for bulb-to-bulb distillation. 1: Still pot with stirrer bar/anti-bumping granules 2: Cold finger - Condenser with maximum surface to condense most of the vapour. 3: Cooling water outlet 4: cooling water inlet 5: Vacuum Adapter 6: Receiving Flask.
Short-path distillation is a distillation technique that involves the distillate traveling a short distance, often only a few centimeters, and is normally done at reduced pressure. [ 1 ] [ 2 ] Short-path distillation systems often have a variety of names depending on the manufacturer of the system and what compounds are being distilled within them.
Originally designed for concentrating sugar in sugar cane juice, it has since become widely used in all industrial applications where large volumes of water must be evaporated, such as salt production and water desalination. Multiple-effect evaporation commonly uses sensible heat in the condensate to preheat liquor to be flashed. In practice ...
Aqueous biphasic systems (ABS) or aqueous two-phase systems (ATPS) are clean alternatives for traditional organic-water solvent extraction systems.. ABS are formed when either two polymers, one polymer and one kosmotropic salt, or two salts (one chaotropic salt and the other a kosmotropic salt) are mixed at appropriate concentrations or at a particular temperature.
The other application of the heteroazeotropic distillation is the separation of a binary system (A-B) forming a homogeneous azeotrope. In this case an entrainer or solvent is added to the mixture in order to form an heteroazeotrope with one or both of the components in order to help the separation of the original A-B mixture.
The total evaporation in all the stages is up to approximately 85% of the water flowing through the system, depending on the range of temperatures used. With increasing temperature there are growing difficulties of scale formation and corrosion. 110-120 °C appears to be a maximum, although scale avoidance may require temperatures below 70 °C.
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