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The chiral stationary phase can be prepared by mixing chirally pure reagents such as L-amino acid, or brucine, or a chiral ligand exchange reagent with silica gel slurry, [2] [3] or by impregnation of the TLC plate in the solution of a chiral reagent. [4]
It is performed on a TLC plate made up of a non-reactive solid coated with a thin layer of adsorbent material. [2] This is called the stationary phase. [2] The sample is deposited on the plate, which is eluted with a solvent or solvent mixture known as the mobile phase (or eluent). [3] This solvent then moves up the plate via capillary action. [4]
The spot capacity (analogous to peak capacity in HPLC) can be increased by developing the plate with two different solvents, using two-dimensional chromatography. [8] The procedure begins with development of a sample loaded plate with first solvent. After removing it, the plate is rotated 90° and developed with a second solvent.
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Prevention through design (PtD), also called safety by design usually in Europe, is the concept of applying methods to minimize occupational hazards early in the design process, with an emphasis on optimizing employee health and safety throughout the life cycle of materials and processes. [1]
In chromatography, the retardation factor (R) is the fraction of an analyte in the mobile phase of a chromatographic system. [1] In planar chromatography in particular, the retardation factor R F is defined as the ratio of the distance traveled by the center of a spot to the distance traveled by the solvent front. [2]
Sandwich theory [1] [2] describes the behaviour of a beam, plate, or shell which consists of three layers—two facesheets and one core. The most commonly used sandwich theory is linear and is an extension of first-order beam theory.
In earlier days, birch bark was occasionally used as a flashing material. [7] Most flashing materials today are metal, plastic, rubber, or impregnated paper. [8]Metal flashing materials include lead, aluminium, copper, [1] stainless steel, zinc alloy, other architectural metals or a metal with a coating such as galvanized steel, lead-coated copper, anodized aluminium, terne-coated copper ...