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Gunpowder, also commonly known as black powder to distinguish it from modern smokeless powder, is the earliest known chemical explosive. It consists of a mixture of sulfur , charcoal (which is mostly carbon ), and potassium nitrate (saltpeter) .
Diphenylamine is an organic compound with the formula (C 6 H 5) 2 NH. The compound is a derivative of aniline, consisting of an amine bound to two phenyl groups. The compound is a colorless solid, but commercial samples are often yellow due to oxidized impurities. [5]
Finnish smokeless powder. Smokeless powder is a type of propellant used in firearms and artillery that produces less smoke and less fouling when fired compared to black powder. Because of their similar use, both the original black powder formulation and the smokeless propellant which replaced it are commonly described as gunpowder.
Earliest known written formula for gunpowder, from the Wujing Zongyao of 1044 AD.. Gunpowder is the first explosive to have been developed. Popularly listed as one of the "Four Great Inventions" of China, it was invented during the late Tang dynasty (9th century) while the earliest recorded chemical formula for gunpowder dates to the Song dynasty (11th century).
Most presumptive tests involve a chemical reaction that results in a colour change that is detectable with the plain eye. It is important to note that thorough documentation of the scene through notes, photographs etc. must be done prior to any presumptive or confirmatory testing in order to maintain chain of custody and avoid contamination.
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The Wujing Zongyao's first recorded gunpowder formula used in these bombs held a potassium nitrate level of 55.4% to 55.5%, sulfur content of 19.4% to 26.5%, and carbonaceous content of 23% to 25.2%. [34] The first step for making gunpowder is to powder and mix together sulphur, saltpetre, charcoal, pitch, and dried lacquer.
In precise chemical terms, nitrocellulose is not a nitro compound, but a nitrate ester. The glucose repeat unit (anhydroglucose) within the cellulose chain has three OH groups, each of which can form a nitrate ester. Thus, nitrocellulose can denote mononitrocellulose, dinitrocellulose, and trinitrocellulose, or a mixture thereof.