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Free Induction Decay (FID) nuclear magnetic resonance signal seen from a well shimmed sample. In NMR and MRI, shimming is used prior to the operation of the magnet to eliminate inhomogeneities in its field. Initially, the magnetic field inside an NMR spectrometer or MRI scanner will be far from homogeneous compared with an "ideal" field of the ...
Free induction decay (FID) nuclear magnetic resonance signal seen from a well shimmed sample. In Fourier transform nuclear magnetic resonance spectroscopy, free induction decay (FID) is the observable nuclear magnetic resonance (NMR) signal generated by non-equilibrium nuclear spin magnetization precessing about the magnetic field (conventionally along z).
In nuclear magnetic resonance spectroscopy, "shimming an NMR magnet" is a procedure to generate homogeneous magnetic field along the sample volume to obtain pure Lorentzian line shapes of various resonances in the spectrum. This is accomplished by manual shimming of individual shims, or automatic shimming procedure. [5]
Nuclear magnetic resonance (NMR) spectroscopy uses the intrinsic magnetic moment that arises from the spin angular momentum of a spin-active nucleus. [1] If the element of interest has a nuclear spin that is not zero, [1] the nucleus may exist in different spin angular momentum states, where the energy of these states can be affected by an external magnetic field.
Paramagnetic nuclear magnetic resonance spectroscopy refers to nuclear magnetic resonance (NMR) spectroscopy of paramagnetic compounds. [1] [2] Although most NMR measurements are conducted on diamagnetic compounds, paramagnetic samples are also amenable to analysis and give rise to special effects indicated by a wide chemical shift range and broadened signals.
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Available through Wiley Online Library [3] (John Wiley & Sons), SpecInfo on the Internet NMR is a collection of approximately 440,000 NMR spectra (organized as 13 C, 1 H, 19 F, 31 P, and 29 Si NMR databases). The data are accessed via the Internet using a Java interface and are stored in a server developed jointly with BASF. The software ...