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Oil sampling is a procedure for collecting a volume of fluid from lubricated or hydraulic machinery for the purpose of oil analysis. Much like collecting forensic evidence at a crime scene, when collecting an oil sample, it is important to ensure that procedures are used to minimize disturbance of the sample during and after the sampling process.
The AutoAnalyzer is an automated analyzer using a flow technique called continuous flow analysis (CFA), or more correctly segmented flow analysis (SFA) first made by the Technicon Corporation. The instrument was invented in 1957 by Leonard Skeggs, PhD and commercialized by Jack Whitehead's Technicon Corporation.
Ferrography is a method of oil analysis used to inspect the severity and mechanisms of wear in machinery. This is achieved by separating ferrous debris from lubricating oil by use of a magnetic field with an instrument called a ferrograph, the result is then examined with microscopy. A trained analyst can then diagnose faults or predict failures.
A sample is typically dissolved in a pre-mixed solvent of chlorobenzene and acetic acid and titrated with standardised perchloric acid in glacial acetic acid for fresh oil samples. [2] The end point is detected using a glass electrode which is immersed in an aqueous solution containing the sample, and connected to a voltmeter/potentiometer.
All oil tankers with a gross tonnage of larger than 150 must have efficient Oil Discharge Monitoring Equipment on board. [3] [4] The oily discharge is sent out to sea through a pump. [5] The oily mixture has to pass through a series of sensors to determine whether it is acceptable to be sent to the discharge pipe. [6]
The history of discrete sample analysis for the clinical laboratory began with the introduction of the "Robot Chemist" invented by Hans Baruch and introduced commercially in 1959 [1]. The AutoAnalyzer is an early example of an automated chemistry analyzer using a special flow technique named "continuous flow analysis (CFA)", invented in 1957 by ...
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