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Lead tetrachloride, also known as lead(IV) chloride, has the molecular formula PbCl 4. It is a yellow, oily liquid which is stable below 0 °C, and decomposes at 50 °C. [2] It has a tetrahedral configuration, with lead as the central atom. The Pb–Cl covalent bonds have been measured to be 247 pm and the bond energy is 243 kJ⋅mol −1. [4]
Lead perchlorate trihydrate is produced by the reaction of lead(II) oxide, lead carbonate, or lead nitrate by perchloric acid: . Pb(NO 3) 2 + HClO 4 → Pb(ClO 4) 2 + HNO 3. The excess perchloric acid was removed by first heating the solution to 125 °C, then heating it under moist air at 160 °C to remove the perchloric acid by converting the acid to the dihydrate.
In moist air it turns into green vitriol, FeSO 4. Massicot – lead monoxide. PbO; Litharge – lead monoxide, formed by fusing and powdering massicot. Minium/red lead – trilead tetroxide, Pb 3 O 4; formed by roasting litharge in air. Naples yellow/cassel yellow – oxychloride of lead, formed by heating litharge with sal ammoniac.
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A perchlorate is a chemical compound containing the perchlorate ion, ClO − 4, the conjugate base of perchloric acid (ionic perchlorate).As counterions, there can be metal cations, quaternary ammonium cations or other ions, for example, nitronium cation (NO + 2).
Chlorate is the common name of the ClO − 3 anion, whose chlorine atom is in the +5 oxidation state.The term can also refer to chemical compounds containing this anion, with chlorates being the salts of chloric acid.
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Sodium perchlorate is the precursor to ammonium, potassium and lithium perchlorate salts, often taking advantage of their low solubility in water relative to NaClO 4 (209 g/(100 mL) at 25 °C). [ 6 ] It is used for denaturating proteins in biochemistry and in standard DNA extraction and hybridization reactions in molecular biology .