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Some producers feel that this unbalances their wine, and use spinning cones to reduce the alcohol by 1-2 percentage points. In this case the wine is passed through the column once to distill out the most volatile aroma compounds which are then put to one side while the wine goes through the column a second time at higher temperature to extract ...
A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...
[1] [2] [3] It uses the fact that the composition at each theoretical tray is completely determined by the mole fraction of one of the two components. This method is based on the assumptions that the distillation column is isobaric —i.e the pressure remains constant—and that the flow rates of liquid and vapor do not change throughout the ...
Refining is used primarily in the petroleum industry, whereby crude oil is heated and separated into stages according to the condensation points of the various elements. Distillation, widely used in petroleum refining and in purification of ethanol separates volatile liquids on the basis of their relative volatilities. There are several type of ...
The other bulbs can be used to collect the distillates sequentially, when the desired fraction is being collected the bulb is cooled with water or ice to aid condensation. A motor drive is often used to rotate the string of bulbs to reduce bumping , give even heating, and increase the surface area for evaporation.
This equipment can be used in cases other than simple removal of water. One example is the esterification of butanol with acetic acid catalyzed by sulfuric acid . The vapor contains 63% ester, 29% water and 8% alcohol at reflux temperature and the organic layer in the trap contains 86% ester, 11% alcohol and 3% water which is reintroduced.
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A still uses the same concepts as a basic distillation apparatus, but on a much larger scale. Stills have been used to produce perfume and medicine, water for injection (WFI) for pharmaceutical use, generally to separate and purify different chemicals, and to produce distilled beverages containing ethanol.