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A simple short path vacuum distillation apparatus can be used for bulb-to-bulb distillation. 1: Still pot with stirrer bar/anti-bumping granules 2: Cold finger - Condenser with maximum surface to condense most of the vapour. 3: Cooling water outlet 4: cooling water inlet 5: Vacuum Adapter 6: Receiving Flask.
Büchner flask A Büchner funnel is attached to the flask via a black elastomer adapter. The hose barb is connected via vacuum hose to a vacuum source such as an aspirator. The flask should be clamped before use or the hose will likely cause it to tip. Cross section of a Büchner Flask. Note the hose barb pointing right for attaching a vacuum ...
Other adapters, such as distillation heads and vacuum adapters, are made with joints that fit in with this convention. If a flask or other container has an extra outer ground-glass joint on it, which needs to be closed off for an experiment, there are often conically tapered inner ground-glass stoppers for that purpose.
A vacuum tight seal and stability of the Büchner flask and filter are essential during the filtration process. A Büchner ring can be used with Büchner funnels, flasks, glass crucibles and Gooch crucibles. The wide flange and large surface contact ensures an excellent vacuum tight seal whilst the rings are easy to remove and offer excellent ...
Vacuum distillation or distillation under reduced pressure is a type of distillation performed under reduced pressure, which allows the purification of compounds not readily distilled at ambient pressures or simply to save time or energy. This technique separates compounds based on differences in their boiling points.
The Schlenk line (also vacuum gas manifold) is a commonly used chemistry apparatus developed by Wilhelm Schlenk. [1] It consists of a dual manifold with several ports. [ 2 ] One manifold is connected to a source of purified inert gas , while the other is connected to a vacuum pump .
Diagram of the vacuum filtration apparatus. By flowing through the aspirator, water will suck out the air contained in the vacuum flask and the Büchner flask.There is therefore a difference in pressure between the exterior and the interior of the flasks : the contents of the Büchner funnel are sucked towards the vacuum flask.
A Schlenk flask, or Schlenk tube, is a reaction vessel typically used in air-sensitive chemistry, invented by Wilhelm Schlenk.It has a side arm fitted with a PTFE or ground glass stopcock, which allows the vessel to be evacuated or filled with gases (usually inert gases like nitrogen or argon).
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