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2-Naphthalenethiol is an organosulfur compound with the formula C 10 H 7 SH. It is a white solid. It is a white solid. It is one of two mono thiols of naphthalene , the other being 1-naphthalenethiol .
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Traditionally, 2-naphthol is produced by a two-step process that begins with the sulfonation of naphthalene in sulfuric acid: [2] C 10 H 8 + H 2 SO 4 → C 10 H 7 SO 3 H + H 2 O. The sulfonic acid group is then cleaved in molten sodium hydroxide: C 10 H 7 (SO 3 H) + 3 NaOH → C 10 H 7 ONa + Na 2 SO 3 + 2 H 2 O. Neutralization of the product ...
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[1] 1-Naphthalenethiol can also be prepared from 1-bromonaphthalene by Pd-catalyzed reaction with the silylthiolate i Pr 3 SiSK followed by hydrolysis of the silathioether. [2] It was first prepared from the Grignard reagent generated from 1-bromonaphthalene. Treatment of that reagent with elemental sulfur followed by acidification gave the ...
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