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Recrystallization is a method used to purify chemicals by dissolving a mixture of a compound and its impurities, in an appropriate solvent, prior to heating the solution. [1] Following the dissolution of crude product, the mixture will passively cool, yielding a crystallized compound and its impurities as separate entities.
In a laboratory setting, mixture of dissolved materials are typically fed using a solvent into a column packed with an appropriate adsorbent, and due to different affinities for solvent (moving phase) versus adsorbent (stationary phase) the components in the original mixture pass through the column in the moving phase at different rates, which ...
In materials science, recrystallization is a process by which deformed grains are replaced by a new set of defect-free grains that nucleate and grow until the original grains have been entirely consumed. Recrystallization is usually accompanied by a reduction in the strength and hardness of a material and a simultaneous increase in the ...
A Craig tube is an item of apparatus used in small-scale (up to about 100 mg) preparative and analytical chemistry, particularly for recrystallisation.It was invented by Lyman C. Craig and Otto W. Post. [1]
Pages in category "Laboratory techniques" The following 200 pages are in this category, out of approximately 260 total. ... Recrystallization (chemistry) Reflux;
In metallurgy, materials science and structural geology, subgrain rotation recrystallization is recognized as an important mechanism for dynamic recrystallisation.It involves the rotation of initially low-angle sub-grain boundaries until the mismatch between the crystal lattices across the boundary is sufficient for them to be regarded as grain boundaries.
Often these raw materials must go through a separation before they can be put to productive use, making separation techniques essential for the modern industrial economy. The purpose of separation may be: analytical: to identify the size of each fraction of a mixture is attributable to each component without attempting to harvest the fractions.
Dynamic recrystallization (DRX) is a type of recrystallization process, found within the fields of metallurgy and geology. In dynamic recrystallization, as opposed to static recrystallization, the nucleation and growth of new grains occurs during deformation rather than afterwards as part of a separate heat treatment.