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Short-path distillation is a distillation technique that involves the distillate traveling a short distance, often only a few centimeters, and is normally done at reduced pressure. [ 1 ] [ 2 ] Short-path distillation systems often have a variety of names depending on the manufacturer of the system and what compounds are being distilled within them.
"Short path" refers to the short distance that the vapors of the distillate need to travel, which helps reduce loss and speed up collection of the distillate.This type of distillation is generally performed under vacuum to prevent the compound from charring due to atmospheric oxygen, as well as to allow the distillation to proceed at a lower temperature.
Molecular distillation is a type of short-path vacuum distillation, characterized by an extremely low vacuum pressure, 0.01 torr or below, which is performed using a molecular still. [1] It is a process of separation, purification and concentration of natural products, complex and thermally sensitive molecules for example vitamins and ...
Short path distillation is a distillation technique that involves the distillate travelling a short distance, often only a few centimeters, and is normally done at reduced pressure. [ 1 ] : 150 A classic example would be a distillation involving the distillate travelling from one glass bulb to another, without the need for a condenser ...
Compounds with a boiling point lower than 150 °C typically are distilled at ambient pressure. For samples with high boiling points, short-path distillation apparatus is commonly employed. [3] [4] This technique is amply illustrated in Organic Synthesis. [5] [6]
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