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  2. List of cooling baths - Wikipedia

    en.wikipedia.org/wiki/List_of_cooling_baths

    Dry ice: Tetrachloroethylene-22 Dry ice: Carbon Tetrachloride-23 Dry ice: 1,3-Dichlorobenzene-25 Dry ice: o-Xylene-29 Liquid N 2: Bromobenzene-30 Dry ice: m-Toluidine-32 Dry ice: 3-Heptanone-38 Ice: Calcium chloride hexahydrate -40 1 to 0.8 ratio of salt to ice. Dry ice: Acetonitrile-41 Dry ice: Pyridine-42 Dry ice: Cyclohexanone-46 Dry ice: m ...

  3. Trituration - Wikipedia

    en.wikipedia.org/wiki/Trituration

    In organic chemistry, trituration is a process used to purify crude chemical compounds containing soluble impurities. A solvent is chosen in which the desired product is insoluble and the undesired by-products are very soluble or vice versa. For example, when the impurities are soluble and the desired product is not, the crude material is ...

  4. Drying tube - Wikipedia

    en.wikipedia.org/wiki/Drying_tube

    A variety of empty glass drying tubes. When used, they are packed with a desiccant, usually calcium chloride. A drying tube or guard tube is a tube-like piece of apparatus used to house a disposable solid desiccant, wherein at one end the tube-like structure terminates in a ground glass joint for use in connecting the drying tube to a reaction vessel, for the purpose of keeping the vessel free ...

  5. Anhydrous - Wikipedia

    en.wikipedia.org/wiki/Anhydrous

    Organic solutions can be dried using a range of drying agents. Typically following a workup the organic extract is dried using magnesium sulfate or a similar drying agent to remove most remaining water. [5] Anhydrous acetic acid is known as glacial acetic acid.

  6. Wet chemistry - Wikipedia

    en.wikipedia.org/wiki/Wet_chemistry

    Wet chemistry is a form of analytical chemistry that uses classical methods such as observation to analyze materials. The term wet chemistry is used as most analytical work is done in the liquid phase. [1] Wet chemistry is also known as bench chemistry, since many tests are performed at lab benches. [2]

  7. Drying - Wikipedia

    en.wikipedia.org/wiki/Drying

    Vacuum microwave drying is used for the US Army's experimental Close Combat Assault Ration. [3] Freeze drying or lyophilization is a drying method where the solvent is frozen prior to drying and is then sublimed, i.e., passed to the gas phase directly from the solid phase, below the melting point of the solvent. It is increasingly applied to ...

  8. Column chromatography - Wikipedia

    en.wikipedia.org/wiki/Column_chromatography

    The solutions and buffers pass through the column where a fraction collector at the end of the column setup collects the eluted samples. Prior to the fraction collection, the samples that are eluted from the column pass through a detector such as a spectrophotometer or mass spectrometer so that the concentration of the separated samples in the ...

  9. Acid–base extraction - Wikipedia

    en.wikipedia.org/wiki/Acid–base_extraction

    Acid–base extraction is a subclass of liquid–liquid extractions and involves the separation of chemical species from other acidic or basic compounds. [1] It is typically performed during the work-up step following a chemical synthesis to purify crude compounds [2] and results in the product being largely free of acidic or basic impurities.