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Sample preparation may involve dissolution, extraction, reaction with some chemical species, pulverizing, treatment with a chelating agent (e.g. EDTA), masking, filtering, dilution, sub-sampling or many other techniques. Treatment is done to prepare the sample into a form ready for analysis by specified analytical equipment.
Samples prepared using the QuEChERS method can be processed more quickly using a homogenization instrument. [citation needed] Such instruments can homogenize the food sample in a centrifuge tube, then agitate the sample with the reagent of choice, before moving the extracted sample for centrifuging. By using such an instrument, the samples can ...
There are exceptions, however, such as the sampling of nut products for the presence of aflatoxins, which stipulate a primary sample size related to the size of the consignment – with associated requirements for initial homogenisation to produce a smaller sample to be sent for analysis. The Food Safety Act 1990 [1] affords a right for defence ...
Microwave digestion is a chemical technique used to decompose sample material into a solution suitable for quantitative elemental analysis. [1] It is commonly used to prepare samples for analysis using inductively coupled plasma mass spectrometry (ICP-MS), atomic absorption spectroscopy, and atomic emission spectroscopy (including ICP-AES).
A measurement system analysis (MSA) is a thorough assessment of a measurement process, and typically includes a specially designed experiment that seeks to identify the components of variation in that measurement process. Just as processes that produce a product may vary, the process of obtaining measurements and data may also have variation ...
The Dumas technique has been automated and instrumentalized, so that it is capable of rapidly measuring the crude protein concentration of food samples. This automatic Dumas technique has replaced the Kjeldahl method as the standard method of analysis for nutritional labelling of protein content of foods (except in high fat content foods where ...
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It could also arise as a result of pouring the milk sample directly onto the acid in the butyrometer. To avoid charring, first, ensure the acid concentration is right. Secondly, while adding the milk sample, let it flow on the side of the butyrometer to avoid violent reaction when it drops on the surface of the acid.