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Distillation using semi-microscale apparatus. The jointless design eliminates the need to fit pieces together. The pear-shaped flask allows the last drop of residue to be removed, compared with a similarly sized round-bottom flask. The small holdup volume prevents losses. A "pig" is used to channel the various distillates into three receiving ...
Flat-bottomed flask: A flask with similar uses as the round-bottom flask, but with a flat bottom that allows it to stand on a level surface. Florence flask: A flask similar to the flat-bottomed flask that has round bodies and either a round bottom or a flat bottom so that one can stand the flask on a level surface. Florence flasks typically ...
Volumetric flask is used for preparing liquids with volumes of high precision. It is a flask with an approximately pear-shaped body and a long neck with a circumferential fill line. Dewar flask is a double-walled flask having a near-vacuum between the two walls. These come in a variety of shapes and sizes; some are large and tube-like, others ...
A Florence flask/boiling flask is a type of flask used as an item of laboratory glassware and is named after the city Florence. [1] It is used as a container to hold liquids. A Florence flask has a round body, a long neck, and often a flat botto
The Marcusson apparatus, Dean-Stark apparatus, Dean–Stark receiver, distilling trap, or Dean–Stark Head is a piece of laboratory glassware used in synthetic chemistry to collect water [1] [2] (or occasionally other liquid) from a reactor. It is used in combination with a reflux condenser and a distillation flask for the separation of water ...
Fractional distillation in a laboratory makes use of common laboratory glassware and apparatuses, typically including a Bunsen burner, a round-bottomed flask and a condenser, as well as the single-purpose fractionating column. Fractional distillation. As an example, consider the distillation of a mixture of water and ethanol. Ethanol boils at ...
The solvent is returned to the distillation flask. The thimble ensures that the rapid motion of the solvent does not transport any solid material to the still pot. This cycle may be allowed to repeat many times, over hours or days. During each cycle, a portion of the non-volatile compound dissolves in the solvent. After many cycles the desired ...
In a typical fractional distillation, a liquid mixture is heated in the distilling flask, and the resulting vapor rises up the fractionating column (see Figure 1). The vapor condenses on glass spurs (known as theoretical trays or theoretical plates) inside the column, and returns to the distilling flask, refluxing the rising distillate vapor ...
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