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Porosimetry is an analytical technique used to determine various quantifiable aspects of a material's porous structure, such as pore diameter, total pore volume, surface area, and bulk and absolute densities. The technique involves the intrusion of a non-wetting liquid (often mercury) at high pressure into a material through the use of a ...
Powder wettability measurement with the Washburn method. In its most general form the Lucas Washburn equation describes the penetration length of a liquid into a capillary pore or tube with time as = (), where is a simplified diffusion coefficient. [4]
In capillary flow porometry, in opposition to mercury intrusion porosimetry, the wetting liquid enters spontaneously the pores of the sample ensuring a total wetting of the material, and therefore the contact angle of the wetting liquid with the sample is 0 and the previous formula can be simplified as: P= 4*γ/D.
Micro CT of porous medium: Pores of the porous medium shown as purple color and impermeable porous matrix shown as green-yellow color. Pore structure is a common term employed to characterize the porosity, pore size, pore size distribution, and pore morphology (such as pore shape, surface roughness, and tortuosity of pore channels) of a porous medium.
However, simple cooling of an all-liquid sample usually leads to a state of non-equilibrium super cooling and only eventual non-equilibrium freezing – to obtain a measurement of the equilibrium freezing event, it is necessary to first cool enough to freeze a sample with excess liquid outside the pores, then warm the sample until the liquid in ...
A sample of known bulk volume is enclosed in a container of known volume. It is connected to another container with a known volume which is evacuated (i.e., near vacuum pressure). When a valve connecting the two containers is opened, gas passes from the first container to the second until a uniform pressure distribution is attained.
[1] [3] The sample is immersed for some time in 2-propanol prior to measurement to ensure saturation of pores, and is then placed into the cell in an analytical balance and immersed again in 2-propanol, after which the change in mass due to evaporation of the free-standing liquid layer and then draining of liquid from pores is measured by the ...
A detailed analysis of the shape of these isotherms is done using the Kelvin equation. This enables the pore size distribution to be determined. [2] While this is a relatively simple method of analyzing the isotherms, a more in depth analysis of the isotherms is done using the BET method. Another method of determining the pore size distribution ...
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