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2 CH 3 Cl + Si → (CH 3) 4−n SiCl n + other products. While this reaction is the standard in industrial silicone production and is nearly identical to the first direct synthesis of methyltrichlorosilane, the overall process is inefficient with respect to methyltrichlorosilane. [2]
Methyltrichlorosilane can be used to induce branching and cross-linking in PDMS molecules, while chlorotrimethylsilane serves to end backbone chains, limiting molecular weight. Other acid-forming species, especially acetate, can replace chlorine in silicone synthesis with little difference in the chemistry of the finished polymer. These ...
Methyltrimethoxysilane is usually prepared from methyltrichlorosilane and methanol: CH 3 SiCl 3 + 3 CH 3 OH → CH 3 Si(OCH 3) 3 + 3 HCl. Alcoholysis of alkylchlorosilanes typically proceeds via an S N 2 mechanism. Inversion of the configuration is favored during nucleophilic attack when displacing good leaving groups, such as chloride. [3]
The more useful products of this reaction are those for x = 1 (trimethylsilyl chloride), 2 (dimethyldichlorosilane), and 3 (methyltrichlorosilane). [1] TMS undergoes deprotonation upon treatment with butyllithium to give (H 3 C) 3 SiCH 2 Li. The latter, trimethylsilylmethyl lithium, is a relatively common alkylating agent.
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This also includes water, potentially producing silicon dioxide, chlorine, hydrogen, hydrogen chloride (and its aqueous form hydrochloric acid), and heat. Trichlorosilane can cause hazardous chemical reactions with moisture and humidity alone, and should be handled and stored under inert gas . [ 8 ]
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