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Crystallization is the process by which solids form, where the atoms or molecules are highly organized into a structure known as a crystal.Some ways by which crystals form are precipitating from a solution, freezing, or more rarely deposition directly from a gas.
In chemistry, fractional crystallization is a stage-wise separation technique that relies on the liquid–solid phase change. This technique fractionates via differences in crystallization temperature and enables the purification of multi-component mixtures, as long as none of the constituents can act as solvents to the others. Due to the high ...
For other solvents of crystallization, analysis is conveniently accomplished by dissolving the sample in a deuterated solvent and analyzing the sample for solvent signals by NMR spectroscopy. Single crystal X-ray crystallography is often able to detect the presence of these solvents of crystallization as well. Other methods may be currently ...
The unit cell is defined as the smallest repeating unit having the full symmetry of the crystal structure. [2] The geometry of the unit cell is defined as a parallelepiped , providing six lattice parameters taken as the lengths of the cell edges ( a , b , c ) and the angles between them (α, β, γ).
Crystallization of polymers is a process associated with partial alignment of their molecular chains. These chains fold together and form ordered regions called lamellae , which compose larger spheroidal structures named spherulites .
Crystal chemistry is the study of the principles of chemistry behind crystals and their use in describing structure-property relations in solids, as well as the chemical properties of periodic structures. [1]
Phase transitions (phase changes) that help describe polymorphism include polymorphic transitions as well as melting and vaporization transitions. According to IUPAC, a polymorphic transition is "A reversible transition of a solid crystalline phase at a certain temperature and pressure (the inversion point) to another phase of the same chemical composition with a different crystal structure."
Crystals found in rocks typically range in size from a fraction of a millimetre to several centimetres across, although exceptionally large crystals are occasionally found. As of 1999 [update] , the world's largest known naturally occurring crystal is a crystal of beryl from Malakialina, Madagascar , 18 m (59 ft) long and 3.5 m (11 ft) in ...