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The oil level is a little low now to compensate for expansion when heating commences. The Thiele tube, named after the German chemist Johannes Thiele, is a laboratory glassware designed to contain and heat an oil bath. Such a setup is commonly used in the determination of the melting point or boiling point of a substance.
The sample is then heated, either by a heating block or an oil bath, and as the temperature increases, the sample is observed to determine when the phase change from solid to liquid occurs. The operator of the apparatus records the temperature range starting with the initial phase-change temperature and ending with the completed phase-change ...
Mineral oil cannot be used above 310 °C (590 °F) due to the compound's boiling point. If higher temperatures are needed, a silicone oil or a sand bath may be used instead. [2] [better source needed] Silicone oil baths are effective in the 25 °C (77 °F) - 230 °C (446 °F) range. Sand baths are effective from 25 °C (77 °F) to above 500 °C ...
A bain-marie (English: / ˌ b æ n m ə ˈ r iː / BAN-mə-REE, French: [bɛ̃ maʁi]), also known as a water bath or double boiler, a type of heated bath, is a piece of equipment used in science, industry, and cooking to heat materials gently or to keep materials warm over a period of time. A bain-marie is also used to melt ingredients for ...
A heated bath is used in the laboratory to allow a chemical reaction to occur at an elevated temperature. [1] In contrast to traditional Bunsen burners, heated baths use liquids to transfer heat to the reaction vessel. This is achieved using a high-boiling point liquid inside a thermally conducting bath (usually made of metal).
A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...
Round-bottom flasks are often used to contain chemical reactions run by chemists, especially for reflux set-ups and laboratory-scale synthesis. [3] Boiling chips are added in distilling flasks for distillations or boiling chemical reactions to allow a nucleation site for gradual boiling. This nucleation avoids a sudden boiling surge where the ...
A boiling tube is essentially a scaled-up test tube, being about 50% larger. They are designed to be wide enough to allow substances to boil violently as opposed to a test tube, which is too narrow; a boiling liquid can explode out of the end of test tubes when they are heated, as there is no room for bubbles of gas to escape independently of ...