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The method of extractive distillation uses a separation solvent, which is generally non-volatile, has a high boiling point and is miscible with the mixture, but doesn't form an azeotropic mixture. The solvent interacts differently with the components of the mixture thereby causing their relative volatilities to change.
A vapor-compression evaporator, like most evaporators, can make reasonably clean water from any water source. In a salt crystallizer, for example, a typical analysis of the resulting condensate shows a typical content of residual salt not higher than 50 ppm or, in terms of electrical conductance , not higher than 10 μS/cm .
A Perkin triangle is a specialized apparatus for the distillation of air-sensitive materials. Some compounds have high boiling points and are sensitive to air. A simple vacuum distillation system can be used, whereby the vacuum is replaced with an inert gas after the distillation is complete. However, this is a less satisfactory system if one ...
The pressure in the system must be maintained from the pump right through the pressure vessel. In smaller systems (up to about 10 mL / min) a simple restrictor can be used. This can be either a capillary tube cut to length, or a needle valve which can be adjusted to maintain pressure at different flow rates.
A separatory funnel used for liquid–liquid extraction, as evident by the two immiscible liquids.. Liquid–liquid extraction, also known as solvent extraction and partitioning, is a method to separate compounds or metal complexes, based on their relative solubilities in two different immiscible liquids, usually water (polar) and an organic solvent (non-polar).
Laboratory distillation set-up using, without a ... 4: Thermometer/Boiling point temperature 5: Condenser 6: Cooling water in 7: Cooling water out 8 ...
Short-path distillation is a distillation technique that involves the distillate traveling a short distance, often only a few centimeters, and is normally done at reduced pressure. [ 1 ] [ 2 ] Short-path distillation systems often have a variety of names depending on the manufacturer of the system and what compounds are being distilled within them.
Condensers with forced-circulation cooling usually employ water as the cooling fluid. The flow may be open, from a tap to a sink, and driven only by the water pressure in the tap. Alternatively, a closed system may be used, in which the water is drawn by a pump from a tank, possibly refrigerated, and returned to it. Water-cooled condensers are ...