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The thermal conductivity detector (TCD), also known as a katharometer, is a bulk property detector and a chemical specific detector commonly used in gas chromatography. [1] This detector senses changes in the thermal conductivity of the column eluent and compares it to a reference flow of carrier gas. Since most compounds have a thermal ...
Portable instruments for the analysis of helium content of breathing gas mixtures may be based on a thermal conductivity sensor (katharometer). These sensors can be very stable and maintenance free and also highly reliable and accurate. [1] A typical thermal helium analyser comprises two chambers, each with an identical thermal conductivity sensor.
The transient hot wire method has advantage over the other thermal conductivity methods, since there is a fully developed theory and there is no calibration or single-point calibration. Furthermore, because of the very small measuring time (1 s) there is no convection present in the measurements and only the thermal conductivity of the fluid is ...
Dissolved gas analysis (DGA) is an examination of electrical transformer oil contaminants. [1] Insulating materials within electrical equipment liberate gases as they slowly break down over time. The composition and distribution of these dissolved gases are indicators of the effects of deterioration, such as pyrolysis or partial discharge , and ...
Thermal conduction property of any gas under standard conditions of pressure and temperature is a fixed quantity. This property of a known reference gas or known reference gas mixtures can, therefore, be used for certain sensory applications, such as the thermal conductivity analyzer.
The heat generated dissipates into the sample on both sides of the sensor, at a rate depending on the thermal transport properties of the material. By recording temperature vs. time response in the sensor, the thermal conductivity, thermal diffusivity and specific heat capacity of the material can be calculated.
Thermogravimetric analysis or thermal gravimetric analysis (TGA) is a method of thermal analysis in which the mass of a sample is measured over time as the temperature changes. . This measurement provides information about physical phenomena, such as phase transitions, absorption, adsorption and desorption; as well as chemical phenomena including chemisorptions, thermal decomposition, and ...
The information gathered can even be enhanced by coupling the simultaneous thermal analysis instrument to an Evolved Gas Analyzer like Fourier transform infrared spectroscopy or mass spectrometry. Other, less common, methods measure the sound or light emission from a sample, or the electrical discharge from a dielectric material, or the ...
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