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Tungsten hexachloride is an inorganic chemical compound of tungsten and chlorine with the chemical formula W Cl 6. This dark violet-blue compound exists as volatile crystals under standard conditions. It is an important starting reagent in the preparation of tungsten compounds. [1]
An infrared spectroscopy correlation table (or table of infrared absorption frequencies) is a list of absorption peaks and frequencies, typically reported in wavenumber, for common types of molecular bonds and functional groups.
In the initial report, the IR spectroscopy results were interpreted in terms of an octahedral structure. In 1978, a study using photoelectron spectroscopy appeared to confirm the initial assignment of an O h structure. [5] The octahedral assignment remained for nearly 20 years until 1989 when Girolami and Morse showed that [Zr(CH 3) 6] 2−
Infrared spectroscopy (IR spectroscopy or vibrational spectroscopy) is the measurement of the interaction of infrared radiation with matter by absorption, emission, or reflection. It is used to study and identify chemical substances or functional groups in solid, liquid, or gaseous forms. It can be used to characterize new materials or identify ...
Fourier transform infrared spectroscopy (FTIR) [1] is a technique used to obtain an infrared spectrum of absorption or emission of a solid, liquid, or gas. An FTIR spectrometer simultaneously collects high-resolution spectral data over a wide spectral range.
The material is prepared by reduction of tungsten hexachloride. One method involves the use of tetrachloroethylene as the reductant [2] 2 WCl 6 + C 2 Cl 4 → W 2 Cl 10 + C 2 Cl 6. The blue green solid is volatile under vacuum and slightly soluble in nonpolar solvents. The compound is oxophilic and is highly reactive toward Lewis bases.
A hexachloride is a compound or ion that contains six chlorine atoms or ions. It is the highest chloride that an element can form. Common hexachlorides include: Molybdenum hexachloride, MoCl 6; Tungsten hexachloride, WCl 6; Rhenium hexachloride, ReCl 6; Uranium hexachloride, UCl 6; Some hexachloroanions are also known: Hexachloroaluminate [AlCl ...
Tungsten-halogen lamps are frequently used as a near-infrared light source in Infrared spectroscopy. Halogen lamps were used on the Times Square Ball from 1999 to 2006. However, from 2007 onward, the halogen lamps were replaced with LEDs, due to the much longer lifespan, about ten times longer for LED over incandescent. [32]