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13 C NMR Spectrum of DMSO-d 6. Pure deuterated DMSO shows no peaks in 1 H NMR spectroscopy and as a result is commonly used as an NMR solvent. [2] However commercially available samples are not 100% pure and a residual DMSO-d 5 1 H NMR signal is observed at 2.50ppm (quintet, J HD =1.9Hz). The 13 C chemical shift of DMSO-d 6 is 39.52ppm (septet ...
Dimethyl sulfite is prepared from a 1:2 ratio of thionyl chloride and methanol. [4] The reaction can be catalyzed by tertiary amine bases and likely proceeds via the chlorosulfinate (MeOS(O)Cl), [5] this intermediate will exist only fleetingly in the presence of methanol and as such its decomposition to methyl chloride and sulfur dioxide (via the slower SNi mechanism) is not observed to any ...
This style of mixer cleans well between batches, and is favoured for coloured concrete, smaller batches (typically 0.75–3 m 3 or 0.98–3.92 cu yd), and multiple discharge points. Within this category, the pan mixers are losing popularity to the more efficient planetary (or counter-current) mixers, [ 6 ] as the additional mixing action helps ...
Samples were prepared by dissolution in CDCl 3, D 2 O, or DMSO-d 6. [5] Each spectrum is accompanied by a list of the observed peaks with their respective chemical shifts in ppm and their intensities. Most spectra show the peak assignment. This collection contains ca 14,200 spectra and is being updated. [4]
Displayed structural formula of deuterated DMSO (deuterated dimethyl sulfoxide). Created using ACD/ChemSketch 10.0 and Inkscape. Date: 17 April 2007: Source: Own work: Author: Fvasconcellos 20:45, 17 April 2007 (UTC) Permission (Reusing this file)
Deuterated solvents are a group of compounds where one or more hydrogen atoms are substituted by deuterium atoms. These isotopologues of common solvents are often used in nuclear magnetic resonance spectroscopy .
Index of refraction, [1] n D: 1.4795 at 20 °C 1.4787 at 21 °C Abbe number? Dielectric constant, [2] ε r: 48 ε 0 at 20 °C Bond strength? Bond length? Bond angle? Magnetic susceptibility? Surface tension [2] 43 dyn/cm at 20 °C Viscosity: 2.14 mPa·s [2] at 20 °C 1.1 mPa·s [1] at 27 °C
Deuterated DMF; Deuterated DMSO; Deuterated ethanol; Deuterated methanol; Deuterated THF; H. Heavy water This page was last edited on 21 April 2024, at 00:15 (UTC ...
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