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Diagram of a vacuum flask Gustav Robert Paalen, Double Walled Vessel. Patent 27 June 1908, published 13 July 1909 Patent 27 June 1908, published 13 July 1909 The vacuum flask was designed and invented by Scottish scientist James Dewar in 1892 as a result of his research in the field of cryogenics and is sometimes called a Dewar flask in his honour.
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In other cases, a purge-cycle technique is often employed, where the closed, reaction vessel connected to the line is filled with inert gas, evacuated with the vacuum and then refilled. This process is repeated 3 or more times to make sure air is rigorously removed. Moisture can be removed by heating the reaction vessel with a heat gun. [5]
No refrigeration unit is needed for the storage vessel because the liquid oxygen remains cold due to the efficiency of the vacuum container and the loss of latent heat as oxygen vaporizes. Nevertheless, if no oxygen is used the temperature of the storage vessel gradually rises until after about a week the oxygen pressure causes excess oxygen to ...
Straus flasks are distinct from "solvent pots", which are flasks that contain a solvent as well as drying agents. Solvent pots are not usually bombs, or even Schlenk flasks in the classic sense. The most common configuration of a solvent pot is a simple round bottom flask attached to a 180° adapter fitted with some form of valve.
In laboratory and other scientific settings, they are usually referred to simply as flasks. Flasks come in a number of shapes and a wide range of sizes, but a common distinguishing aspect in their shapes is a wider vessel "body" and one (or sometimes more) narrower tubular sections at the top called necks which have an opening at the top.
Cross section of a Büchner Flask. Note the hose barb pointing right for attaching a vacuum source. A Büchner flask, also known as a vacuum flask, [1] filter flask, suction flask, side-arm flask, or Bunsen flask, is a thick-walled Erlenmeyer flask with a short glass tube and hose barb protruding about an inch from its neck.