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Steam distillation is a separation process that consists of distilling water together with other volatile and non-volatile components. The steam from the boiling water carries the vapor of the volatiles to a condenser ; both are cooled and return to the liquid or solid state, while the non-volatile residues remain behind in the boiling container.
For the binary distillation depicted in Figure 1, the required number of theoretical plates is 6. Constructing a McCabe–Thiele diagram is not always straightforward. In continuous distillation with a varying reflux ratio, the mole fraction of the lighter component in the top part of the distillation column will decrease as the reflux ratio ...
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Fractional distillation in a laboratory makes use of common laboratory glassware and apparatuses, typically including a Bunsen burner, a round-bottomed flask and a condenser, as well as the single-purpose fractionating column. Fractional distillation. As an example, consider the distillation of a mixture of water and ethanol. Ethanol boils at ...
A simple vacuum distillation system as exemplified above can be used, whereby the vacuum is replaced with an inert gas after the distillation is complete. However, this is a less satisfactory system if one desires to collect fractions under a reduced pressure.
Short-path distillation is a distillation technique that involves the distillate traveling a short distance, often only a few centimeters, and is normally done at reduced pressure. [ 1 ] [ 2 ] Short-path distillation systems often have a variety of names depending on the manufacturer of the system and what compounds are being distilled within them.
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Salt-effect distillation is a method of extractive distillation in which a salt is dissolved in the mixture of liquids to be distilled. The salt acts as a separating agent by raising the relative volatility of the mixture and by breaking any azeotropes that may otherwise form.