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Nylon 66 is synthesized by polycondensation of hexamethylenediamine and adipic acid. Equivalent amounts of hexamethylenediamine and adipic acid are combined in water. In the original implementation, the resulting ammonium/carboxylate salt was isolated and then heated either in batches or continuously to induce polycondensation.
Hexamethylenediamine or hexane-1,6-diamine, is the organic compound with the formula H 2 N(CH 2) 6 NH 2. The molecule is a diamine, consisting of a hexamethylene hydrocarbon chain terminated with amine functional groups. The colorless solid (yellowish for some commercial samples) has a strong amine odor.
Adipic acid or hexanedioic acid is the organic compound with the formula (CH 2) 4 (COOH) 2. From an industrial perspective, it is the most important dicarboxylic acid : about 2.5 billion kilograms of this white crystalline powder are produced annually, mainly as a precursor for the production of nylon .
It is a clear brown liquid. It reacts with water to give adipic acid. It is prepared by treatment of adipic acid with thionyl chloride. [1] Adipoyl chloride reacts with hexamethylenediamine to form nylon 6,6. [2]
The simplest case refers to the formation of a strictly linear polymer by the reaction (usually by condensation) of two monomers in equimolar quantities. An example is the synthesis of nylon-6,6 whose formula is [−NH−(CH 2) 6 −NH−CO−(CH 2) 4 −CO−] n from one mole of hexamethylenediamine, H 2 N(CH 2) 6 NH 2, and one mole of adipic acid, HOOC−(CH 2) 4 −COOH.
low crystallinity: PAMXD6 made from m-xylylenediamine and adipic acid; amorphous: PA6I made from hexamethylenediamine and isophthalic acid. According to this classification, PA66, for example, is an aliphatic semi-crystalline homopolyamide.
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On February 28, 1935, Gerard Berchet, under the direction of Carothers, produced a half-ounce of polymer from hexamethylenediamine and adipic acid, creating polyamide 6-6, the substance that would come to be known as Nylon. [30]