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These flasks have two vacuum sections. The inner flask contains liquid helium and the outer flask contains liquid nitrogen, with one vacuum section in between. The loss of precious helium is limited in this way. Other improvements to the vacuum flask include the vapour-cooled radiation shield and the vapour-cooled neck, [11] both of which help ...
Cross section of a Büchner Flask. Note the hose barb pointing right for attaching a vacuum source. A Büchner flask, also known as a vacuum flask, [1] filter flask, suction flask, side-arm flask, or Bunsen flask, is a thick-walled Erlenmeyer flask with a short glass tube and hose barb protruding about an inch from its neck.
It is a flask with an approximately pear-shaped body and a long neck with a circumferential fill line. Dewar flask is a double-walled flask having a near-vacuum between the two walls. These come in a variety of shapes and sizes; some are large and tube-like, others are shaped like regular flasks.
A cryogenic storage dewar (or simply dewar) is a specialised type of vacuum flask used for storing cryogens (such as liquid nitrogen or liquid helium), whose boiling points are much lower than room temperature. It is named after inventor James Dewar, who developed it for his own work. They are commonly used in low-temperature physics and chemistry.
Diagram of the vacuum filtration apparatus. By flowing through the aspirator, water will suck out the air contained in the vacuum flask and the Büchner flask.There is therefore a difference in pressure between the exterior and the interior of the flasks : the contents of the Büchner funnel are sucked towards the vacuum flask.
It is often used in combination with a Büchner flask, Büchner ring and sinter seals. A vacuum tight seal and stability of the Büchner flask and filter are essential during the filtration process. A Büchner ring can be used with Büchner funnels, flasks, glass crucibles and Gooch crucibles. The wide flange and large surface contact ensures ...
This page was last edited on 29 September 2022, at 12:35 (UTC).; Text is available under the Creative Commons Attribution-ShareAlike 4.0 License; additional terms may apply.
The flask can then be removed from the glove box and taken to a Schlenk line. Once connected to the Schlenk line, the inert gas and/or vacuum can be applied to the flask as required. While the flask is connected to the line under a positive pressure of inert gas, the septum can be replaced with other apparatus, for example a reflux condenser.
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