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Gas chromatography (GC) is a common type of chromatography used in analytical chemistry for separating and analyzing compounds that can be vaporized without decomposition. Typical uses of GC include testing the purity of a particular substance, or separating the different components of a mixture. [ 1 ]
The first on-line coupling of gas chromatography to a mass spectrometer was reported in the late 1950s. [4] [5] An interest in coupling the methods had been suggested as early as December 1954, [6] but conventional recording techniques had too poor temporal resolution.
Pyrolysis–gas chromatography–mass spectrometry is a method of chemical analysis in which the sample is heated to decomposition to produce smaller molecules that are separated by gas chromatography and detected using mass spectrometry. Pyrolysis is the thermal decomposition of materials in an inert atmosphere or a vacuum.
The use of a mass spectrometer as the detector in gas chromatography was developed during the 1950s by Roland Gohlke and Fred McLafferty. [ 13 ] [ 14 ] [ 15 ] The development of affordable and miniaturized computers has helped in the simplification of the use of this instrument, as well as allowed great improvements in the amount of time it ...
Pyrolysis gas chromatography is also used for environmental samples, [8] including fossils. [9] Pyrolysis GC is used in forensic laboratories to analyze evidence found in crime scenes such as paints, adhesives, plastics, synthetic fibres and soil extracts. [10]
It is frequently used as a detector in gas chromatography. The measurement of ions per unit time makes this a mass sensitive instrument. [1] Standalone FIDs can also be used in applications such as landfill gas monitoring, fugitive emissions monitoring and internal combustion engine emissions measurement [2] in stationary or portable instruments.
Others introduced mass spectrometers to gas chromatography in the late 1950s. [29] The work of Martin and Synge also set the stage for high performance liquid chromatography, suggesting that small sorbent particles and pressure could produce fast liquid chromatography techniques. This became widely practical by the late 1960s (and the method ...
Gas chromatography-mass spectrometry (GC-MS) is a two-dimensional chromatography technique that combines the separation technique of gas chromatography with the identification technique of mass spectrometry. GC-MS is the single most important analytical tool for the analysis of volatile and semi-volatile organic compounds in complex mixtures. [7]