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In a laboratory setting, mixture of dissolved materials are typically fed using a solvent into a column packed with an appropriate adsorbent, and due to different affinities for solvent (moving phase) versus adsorbent (stationary phase) the components in the original mixture pass through the column in the moving phase at different rates, which ...
"Short path" refers to the short distance that the vapors of the distillate need to travel, which helps reduce loss and speed up collection of the distillate.This type of distillation is generally performed under vacuum to prevent the compound from charring due to atmospheric oxygen, as well as to allow the distillation to proceed at a lower temperature.
Steam distillation once was a popular laboratory method for purification of organic compounds, but it has been replaced in many such uses by vacuum distillation and supercritical fluid extraction. It is however much simpler and economical than those alternatives, and remains important in certain industrial sectors. [3]
Laboratory methods and techniques, as used in fields like biology, biochemistry, biophysics, chemistry, molecular biology, etc. Wikimedia Commons has media related to Laboratory techniques . Contents
Analytical chemistry consists of classical, wet chemical methods and modern analytical techniques. [2] [3] Classical qualitative methods use separations such as precipitation, extraction, and distillation. Identification may be based on differences in color, odor, melting point, boiling point, solubility, radioactivity or reactivity.
Acid–base extraction is a subclass of liquid–liquid extractions and involves the separation of chemical species from other acidic or basic compounds. [1] It is typically performed during the work-up step following a chemical synthesis to purify crude compounds [2] and results in the product being largely free of acidic or basic impurities.
A separatory funnel, also known as a separation funnel, separating funnel, or colloquially sep funnel, is a piece of laboratory glassware used in liquid-liquid extractions to separate (partition) the components of a mixture into two immiscible solvent phases of different densities. [1]
Analytical chemistry – Study of the separation, identification, and quantification of matter; Chemical process – A method or means of somehow changing one or more chemicals or chemical compounds. High-performance liquid chromatography – Technique in analytical chemistry; Unit operation – Basic step in a process