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Diazonium compounds or diazonium salts are a group of organic compounds sharing a common functional group [R−N + ≡N]X − where R can be any organic group, such as an alkyl or an aryl, and X is an inorganic or organic anion, such as a halide. The parent compound where R is hydrogen, is diazenylium.
The tetrafluoroborate can be obtained from crude benzenediazonium chloride by salt metathesis using tetrafluoroboric acid. [C 6 H 5 N 2]Cl + HBF 4 → [C 6 H 5 N 2]BF 4 + HCl. The tetrafluoroborate is more stable than the chloride. [2]
The first step is the preparation of a benzene diazonium chloride solution, a diazonium salt created from the reaction of aniline with mixed nitric acid and hydrochloric acid. The second step involves adding the solution of the diazonium salt to 2-naphthol, to produce the diazo dye. Sudan I is prone to photodegradation when exposed to light.
Chlorobenzene (abbreviated PhCl) is an aryl chloride and the simplest of the chlorobenzenes, consisting of a benzene ring substituted with one chlorine atom. Its chemical formula is C 6 H 5 Cl. This colorless, flammable liquid is a common solvent and a widely used intermediate in the manufacture of other chemicals.
Benzal chloride is an organic compound with the formula C 6 H 5 CHCl 2. [1] This colourless liquid is a lachrymator and is used as a building block in organic synthesis . Preparation and usage
Form: colorless liquid Stability: Stable, but very flammable Melting point: 5.5 C Water solubility: negligible Specific gravity: 0.87 Principal hazards *** Benzene is a carcinogen (cancer-causing agent). *** Very flammable. The pure material, and any solutions containing it, constitute a fire risk. Safe handling
Diazo compounds have two main Lewis structures in resonance: R 2 >C − –N + ≡N and R 2 >CH=N + =N −. In organic chemistry, the diazo group is an organic moiety consisting of two linked nitrogen atoms at the terminal position.
All three have been synthesized by various routes: 1-Bromo-2-chlorobenzene: from 2-chloroaniline, via diazotization followed by a Sandmeyer reaction [1]; 1-Bromo-3-chlorobenzene: by (3-chlorophenyl)trimethylgermanium by electrophilic substitution [2] [better source needed]