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Liquid N 2: Cyclohexene-104 Liquid N 2: Isooctane-107 Liquid N 2: Ethyl iodide-109 Liquid N 2: Carbon disulfide-110 Liquid N 2: Butyl bromide-112 Liquid N 2: Ethanol-116 Liquid N 2: Ethyl bromide-119 Liquid N 2: Acetaldehyde-124 Liquid N 2: Methylcyclohexane-126 Liquid N 2: n-Propanol-127 Liquid N 2: n-Pentane-131 Liquid N 2: 1,5-Hexadiene-141 ...
Both flasks are submerged in a dry ice/acetone cooling bath (−78 °C) the temperature of which is being monitored by a thermocouple (the wire on the left). A cooling bath or ice bath , in laboratory chemistry practice, is a liquid mixture which is used to maintain low temperatures, typically between 13 °C and −196 °C.
p-Toluenesulfonic acid (PTSA, pTSA, or pTsOH) or tosylic acid (TsOH) is an organic compound with the formula CH 3 C 6 H 4 SO 3 H. It is a white extremely hygroscopic solid that is soluble in water, alcohols, and other polar organic solvents. [6] The CH 3 C 6 H 4 SO 2 group is known as the tosyl group and is often abbreviated as
The first step (called SC-1, where SC stands for Standard Clean) is performed with a solution of (ratios may vary) [2] 5 parts of deionized water; 1 part of ammonia water, (29% by weight of NH 3) 1 part of aqueous H 2 O 2 (hydrogen peroxide, 30%) at 75 or 80 °C [1] typically for 10 minutes. This base-peroxide mixture removes organic residues.
The scope of the Corey-House synthesis is exceptionally broad, and a range of lithium diorganylcuprates (R 2 CuLi, R = 1°, 2°, or 3° alkyl, aryl, or alkenyl) and organyl (pseudo)halides (RX, R = methyl, benzylic, allylic, 1°, or cyclic 2° alkyl, aryl, or alkenyl and X = Br, I, OTs, or OTf; X = Cl is marginal) will undergo coupling as the nucleophilic and electrophilic coupling partners ...
[2] [3] Anhydrous solvents are commercially available from chemical suppliers, and are packaged in sealed containers to maintain dryness. [4] Typically anhydrous solvents will contain approximately 10 ppm of water and will increase in wetness if they are not properly stored. Organic solutions can be dried using a range of drying agents.
A variety of empty glass drying tubes. When used, they are packed with a desiccant, usually calcium chloride. A drying tube or guard tube is a tube-like piece of apparatus used to house a disposable solid desiccant, wherein at one end the tube-like structure terminates in a ground glass joint for use in connecting the drying tube to a reaction vessel, for the purpose of keeping the vessel free ...
Dimethylacetamide (DMAc or DMA) is the organic compound with the formula CH 3 C(O)N(CH 3) 2. This colorless, water-miscible, high-boiling liquid is commonly used as a polar solvent in organic synthesis. DMA is miscible with most other solvents, although it is poorly soluble in aliphatic hydrocarbons.