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Condenser (laboratory) A distillation setup using a Liebig-type condenser (the tilted double-walled tube at the center). A liquid (not visible) in the flask at left is heated by the blue mantle to the boiling point. The vapor is then cooled as it goes through the inner tube of the condenser. There it becomes liquid again, and drips into the ...
Steam distillation is a separation process that consists of distilling water together with other volatile and non-volatile components. The steam from the boiling water carries the vapor of the volatiles to a condenser; both are cooled and return to the liquid or solid state, while the non-volatile residues remain behind in the boiling container.
The reflux system in a typical industrial distillation column. Reflux is a technique involving the condensation of vapors and the return of this condensate to the system from which it originated. It is used in industrial [1] and laboratory [2] distillations. It is also used in chemistry to supply energy to reactions over a long period of time.
Distillation. Laboratory model of a still. 1: The heat source to boil the mixture. 2: round-bottom flask containing the mixture to be boiled. 3: the head of the still. 4: mixture boiling-point thermometer. 5: the condenser of the still. 6: the cooling-water inlet of the condenser. 7: the cooling-water outlet of the condenser.
Fractional distillation in a laboratory makes use of common laboratory glassware and apparatuses, typically including a Bunsen burner, a round-bottomed flask and a condenser, as well as the single-purpose fractionating column. Fractional distillation. As an example, consider the distillation of a mixture of water and ethanol. Ethanol boils at ...
The Marcusson apparatus, Dean-Stark apparatus, Dean–Stark receiver, distilling trap, or Dean–Stark Head is a piece of laboratory glassware used in synthetic chemistry to collect water [1][2] (or occasionally other liquid) from a reactor. It is used in combination with a reflux condenser and a distillation flask for the separation of water ...
In chemical engineering, azeotropic distillation usually refers to the specific technique of adding another component to generate a new, lower-boiling azeotrope that is heterogeneous (e.g. producing two, immiscible liquid phases), such as the example below with the addition of benzene to water and ethanol. This practice of adding an entrainer ...
Fractionating column. A fractionating column or fractional column is equipment used in the distillation of liquid mixtures to separate the mixture into its component parts, or fractions, based on their differences in volatility. Fractionating columns are used in small-scale laboratory distillations as well as large-scale industrial distillations.