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Deuterium is an isotope with spin = 1, unlike hydrogen-1, which has spin = 1/2. The term deuteron NMR, in direct analogy to proton NMR, is also used. [ 2 ] Deuterium NMR has a range of chemical shift similar to proton NMR but with poor resolution, due to the smaller magnitude of the magnetic dipole moment of the deuteron relative to the proton.
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NMR spectroscopy is nucleus specific. Thus, it can distinguish between hydrogen and deuterium. The amide protons in the protein exchange readily with the solvent, and, if the solvent contains a different isotope, typically deuterium, the reaction can be monitored by NMR spectroscopy. How rapidly a given amide exchanges reflects its solvent ...
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To be NMR-active, a nucleus must have a non-zero nuclear spin (I ≠ 0). [8] It is this non-zero spin that enables nuclei to interact with external magnetic fields and show signals in NMR. Atoms with an odd sum of protons and neutrons exhibit half-integer values for the nuclear spin quantum number (I = 1/2, 3/2, 5/2, and so on). These atoms are ...
Thus, deuterium accounts for about 0.0156% by number (0.0312% by mass) of all hydrogen in the ocean: 4.85 × 10 13 tonnes of deuterium – mainly as HOD (or 1 HO 2 H or 1 H 2 HO) and only rarely as D 2 O (or 2 H 2 O) (deuterium oxide, also known as heavy water) – in 1.4 × 10 18 tonnes of water.
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