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Both flasks are submerged in a dry ice/acetone cooling bath (−78 °C) the temperature of which is being monitored by a thermocouple (the wire on the left). A cooling bath or ice bath , in laboratory chemistry practice, is a liquid mixture which is used to maintain low temperatures, typically between 13 °C and −196 °C.
Dry ice: Tetrachloroethylene-22 Dry ice: Carbon Tetrachloride-23 Dry ice: 1,3-Dichlorobenzene-25 Dry ice: o-Xylene-29 Liquid N 2: Bromobenzene-30 Dry ice: m-Toluidine-32 Dry ice: 3-Heptanone-38 Ice: Calcium chloride hexahydrate -40 1 to 0.8 ratio of salt to ice. Dry ice: Acetonitrile-41 Dry ice: Pyridine-42 Dry ice: Cyclohexanone-46 Dry ice: m ...
Another version involves filling the device with a cold material (examples: ice, dry ice or a mixture such as dry ice/acetone or ice/water). [ 1 ] Typically a cold finger is used in a sublimation apparatus , [ 2 ] or can be used as a compact version of a condenser in either reflux reaction or distillation apparatus.
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This is accomplished through the use of a coolant such as liquid nitrogen or a freezing mixture of dry ice in acetone or a similar solvent with a low melting point. Liquid nitrogen is only used when dry ice or other cryogenic approaches will not condense the desired gasses since liquid nitrogen will also condense oxygen.
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