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The Carius halogen method in analytical chemistry is a method for the quantitative determination of halogens in chemical substances. [1]A known mass of an organic compound is heated with fuming nitric acid in the presence of silver nitrate contained in a hard glass tube known as carius tube, in a furnace.
Adsorbable organic halides (AOX) is a measure of the organic halogen load at a sampling site such as soil from a land fill, water, or sewage waste. [1] The procedure measures chlorine, bromine, and iodine as equivalent halogens, but does not measure fluorine levels in the sample.
The Beilstein test is a simple qualitative chemical test for organic halides. It was developed by Friedrich Konrad Beilstein. [1] A copper wire is cleaned and heated in a Bunsen burner flame to form a coating of copper(II) oxide. It is then dipped in the sample to be tested and once again heated in a flame.
The method electrochemical fluorination is used commercially for the production of perfluorinated compounds. It generates small amounts of elemental fluorine in situ from hydrogen fluoride. The method avoids the hazards of handling fluorine gas. Many commercially important organic compounds are fluorinated using this technology.
The Carius halogen method measures halides quantitatively. [1] Chemical tests for cyanide test for the presence of cyanide, CN −; Copper sulfate tests for the presence of water; Flame tests test for metals; The Gilman test tests for the presence of a Grignard reagent; The Kjeldahl method quantitatively determines the presence of nitrogen
The sodium fusion test, or Lassaigne's test, is used in elemental analysis for the qualitative determination of the presence of foreign elements, namely halogens, nitrogen, and sulfur, in an organic compound. It was developed by J. L. Lassaigne. [1] The test involves heating the sample with sodium metal, "fusing" it with the sample. A variety ...
Demonstration of tested specimen and IRNDT analysis results. IRNDT (infra-red nondestructive testing) method is suitable for detection and inspection of cracks, defects, cavities, voids and inhomogeneities in material, it is also possible to use the method for inspection of welded joints of metal and plastic parts, inspection of solar cells and solar panels, determination of internal structure ...
A flame test involves introducing a sample of the element or compound to a hot, non-luminous flame and observing the color of the flame that results. [4] The compound can be made into a paste with concentrated hydrochloric acid, as metal halides , being volatile, give better results. [ 5 ]