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The simplest standard distillation apparatus is commonly known as a pot still, consisting of a single heated chamber and a vessel to collect purified alcohol. A pot still incorporates only one condensation, whereas other types of distillation equipment have multiple stages which result in higher purification of the more volatile component ...
Distillation. Laboratory model of a still. 1: The heat source to boil the mixture. 2: round-bottom flask containing the mixture to be boiled. 3: the head of the still. 4: mixture boiling-point thermometre. 5: the condenser of the still. 6: the cooling-water inlet of the condenser. 7: the cooling-water outlet of the condenser.
During first distillation, the pot still (or "wash still") is filled about two-thirds full of a fermented liquid (or wash) with an alcohol content of about 7–12%. [4] [5] [6] In the case of whiskey distillation, the liquid used is a beer, while in the case of brandy production, it is a base wine. The pot still is then heated so that the ...
A simple short path vacuum distillation apparatus can be used for bulb-to-bulb distillation. 1: Still pot with stirrer bar/anti-bumping granules 2: Cold finger - Condenser with maximum surface to condense the most of the vapour. 3: Cooling water outlet 4: cooling water inlet 5: Vacuum Adapter 6: Receiving Flask.
Short-path distillation is a distillation technique that involves the distillate traveling a short distance, often only a few centimeters, and is normally done at reduced pressure. [1][2] Short-path distillation systems often have a variety of names depending on the manufacturer of the system and what compounds are being distilled within them.
In chemical engineering, azeotropic distillation usually refers to the specific technique of adding another component to generate a new, lower-boiling azeotrope that is heterogeneous (e.g. producing two, immiscible liquid phases), such as the example below with the addition of benzene to water and ethanol. Common Equipment used in Azeotropic ...
Possessing distilling equipment without a permit is considered a misdemeanor in Texas and punishable by a fine of $100-$1,000.
Vacuum distillation or distillation under reduced pressure is a type of distillation performed under reduced pressure, which allows the purification of compounds not readily distilled at ambient pressures or simply to save time or energy. This technique separates compounds based on differences in their boiling points.
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