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Acid–base extraction is a subclass of liquid–liquid extractions and involves the separation of chemical species from other acidic or basic compounds. [1] It is typically performed during the work-up step following a chemical synthesis to purify crude compounds [2] and results in the product being largely free of acidic or basic impurities.
The tap-controlled outlet is designed to drain the liquid out of the funnel. On top of the funnel there is a standard taper joint which fits with a ground glass or Teflon stopper. [4] To use a separating funnel, the two phases and the mixture to be separated in solution are added through the top with the stopcock at the bottom closed.
A Büchner funnel is a piece of laboratory equipment used in filtration. [1] It is traditionally made of porcelain , but glass and plastic funnels are also available. On top of the funnel-shaped part there is a cylinder with a fritted glass disc/perforated plate separating it from the funnel.
A funnel for hot filtration Two funnels, A - a simple stemmed funnel. B - a ground glass powder funnel. Plain funnels exist in various dimensions, with longer or shorter necks. Filter funnels have a neck of a thin capillary tube and ribs which increase the filter-papers' effectiveness and thus accelerate the process of filtering. [1]
Laboratory-scale liquid-liquid extraction. Photograph of a separatory funnel in a laboratory scale extraction of 2 immiscible liquids: liquids are a diethyl ether upper phase, and a lower aqueous phase. Soxhlet extractor. Extraction in chemistry is a separation process consisting of the separation of a substance from a matrix. The distribution ...
It is primarily used together with a Büchner funnel fitted through a drilled rubber bung or an elastomer adapter (a Büchner ring) at the neck on top of the flask for the filtration of samples. The Büchner funnel holds the sample isolated from the suction by a layer of filter paper. During filtration, the filtrate enters and is held by the ...
Bottled water dispensers can be top-mounted or bottom-loaded, depending on the design of the model. Bottled water dispensers typically use 11- or 22-liter (5- or 10-gallon) dispensers commonly found on top of the unit. Pressure coolers are a subcategory of water dispensers encompassing drinking water fountains and direct-piping water dispensers ...
It was originally designed for the extraction of a lipid from a solid material. Typically, Soxhlet extraction is used when the desired compound has a limited solubility in a solvent, and the impurity is insoluble in that solvent. It allows for unmonitored and unmanaged operation while efficiently recycling a small amount of solvent to dissolve ...