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A Craig tube is an item of apparatus used in small-scale (up to about 100 mg) preparative and analytical chemistry, particularly for recrystallisation.It was invented by Lyman C. Craig and Otto W. Post. [1]
Recrystallization: In analytical and synthetic chemistry work, purchased reagents of doubtful purity may be recrystallised, e.g. dissolved in a very pure solvent, and then crystallized, and the crystals recovered, in order to improve and/or verify their purity.
Recrystallization is a method used to purify chemicals by dissolving a mixture of a compound and its impurities, in an appropriate solvent, prior to heating the solution. [1] Following the dissolution of crude product, the mixture will passively cool, yielding a crystallized compound and its impurities as separate entities.
In materials science, recrystallization is a process by which deformed grains are replaced by a new set of defect-free grains that nucleate and grow until the original grains have been entirely consumed. Recrystallization is usually accompanied by a reduction in the strength and hardness of a material and a simultaneous increase in the ...
In metallurgy, materials science and structural geology, subgrain rotation recrystallization is recognized as an important mechanism for dynamic recrystallisation.It involves the rotation of initially low-angle sub-grain boundaries until the mismatch between the crystal lattices across the boundary is sufficient for them to be regarded as grain boundaries.
Figure 1: Melting point phase diagram (using the Schroeder – van Laar Equation) of a prototypical diastereomeric system. nb. utility in a solvent mediated crystallization implicitly assumes ideal behaviour (in that changing the solvent will not change the composition of the binary eutectic).
Download as PDF; Printable version; In other projects ... move to sidebar hide. Recrystallization may refer to: Recrystallization (chemistry) Recrystallization ...
Often these raw materials must go through a separation before they can be put to productive use, making separation techniques essential for the modern industrial economy. The purpose of separation may be: analytical: to identify the size of each fraction of a mixture is attributable to each component without attempting to harvest the fractions.