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A sublimatory [1] [2] or sublimation apparatus is equipment, commonly laboratory glassware, for purification of compounds by selective sublimation. In principle, the operation resembles purification by distillation , except that the products do not pass through a liquid phase .
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Closed space sublimation is a method of producing thin-films, esp. cadmium telluride photovoltaics, though it is used for other materials like antimony triselenide. [1] Diagram showing working principle of CSS. It is a type of physical vapor deposition where the substrate to be coated and the source material are held close to one another. They ...
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Its construction and principle of operation is simple. It consists of a titanium filament through which a high current (typically around 40 A) is passed periodically. This current causes the filament to reach the sublimation temperature of titanium, and hence the surrounding chamber walls become coated with a thin film of clean titanium.
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