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In analytical chemistry, sample preparation (working-up) refers to the ways in which a sample is treated prior to its analyses. Preparation is a very important step in most analytical techniques, because the techniques are often not responsive to the analyte in its in-situ form, or the results are distorted by interfering species.
Sample preparation for mass spectrometry is used for the optimization of a sample for analysis in a mass spectrometer (MS). Each ionization method has certain factors that must be considered for that method to be successful, such as volume, concentration , sample phase, and composition of the analyte solution.
A riffle box is a box containing a number (between 3 and 12) of "chutes" - slotted paths through which particles of the sample may slide. The sample is dropped into the top, and the box produces two equally divided subsamples. Riffle boxes are commonly used in mining to reduce the size of crushed rock samples prior to assaying.
The material may be solid, liquid, gas, a material of some intermediate characteristics such as gel or sputum, tissue, organism, or a combination of these.Even if a material sample is not countable as individual items, the quantity of the sample may still be describable in terms of its volume, mass, size, or other such dimensions.
Aseptic sampling is the process of aseptically withdrawing materials used in biopharmaceutical processes for analysis so as not contaminate or alter the sample or the source of the sample. [1] Aseptic samples are drawn throughout the entire biopharmaceutical process (cell culture/fermentation, buffer & media prep, purification, final fill and ...
Cut Bakken Core samples. Although often neglected, core samples always degrade to some degree in the process of cutting the core, handling it, and studying it. Non-destructive techniques are increasingly common, e.g., the use of MRI scanning to characterize grains, pore fluids, pore spaces and their interactions (constituting part of permeability) but such expensive subtlety is likely wasted ...
Liquid scintillation counter. Samples are dissolved or suspended in a "cocktail" containing a solvent (historically aromatic organics such as xylene or toluene, but more recently less hazardous solvents are used), typically some form of a surfactant, and "fluors" or scintillators which produce the light measured by the detector.
In situ electron microscopy is an investigatory technique where an electron microscope is used to watch a sample's response to a stimulus in real time. Due to the nature of the high-energy beam of electrons used to image a sample in an electron microscope, microscopists have long observed that specimens are routinely changed or damaged by the electron beam.