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Bucherer carbazole synthesis. A third method for the synthesis of carbazole is the Graebe–Ullmann reaction. Graebe–Ullmann reaction. In the first step, an N-phenyl-1,2-diaminobenzene (N-phenyl-o-phenylenediamine) is converted into a diazonium salt which instantaneously forms a 1,2,3-triazole. The triazole is unstable and at elevated ...
It is prepared by condensation of chloranil and 3-amino-N-ethylcarbazole. It has a centrosymmetric angular structure. [ 2 ] For many years, the structure was assigned, incorrectly, as having a "linear structure" ( EC no. 228-767-9, CAS RN 6358-30-1) which differ in terms of the carbazole ring fusion .
This page contains tables of azeotrope data for various binary and ternary mixtures of solvents. The data include the composition of a mixture by weight (in binary azeotropes, when only one fraction is given, it is the fraction of the second component), the boiling point (b.p.) of a component, the boiling point of a mixture, and the specific gravity of the mixture.
Melting point: 66 °C (151 °F; 339 K) Boiling point: ... It is produced by the vinylation of carbazole with acetylene in the presence of base. [6] Related compounds
Boiling point (°C) K b (°C⋅kg/mol) Freezing point (°C) K f (°C⋅kg/mol) Data source; ... Ethyl Acetate: 77.1 [5] Acetic Anhydride: 139.0 [6] Ethylene ...
An alternative, innovative and highly promising approach to convert LOHC-bound hydrogen into electricity is proposed recently. [1] The new unloading sequence consists of an almost thermoneutral catalysed transfer hydrogenation step converting ketone to secondary alcohol by contacting hydrogen-rich carrier (H18-DBT), and the secondary alcohol is then directly consumed in a PEMFC (direct ...
Polyvinylcarbazole was discovered by the chemists Walter Reppe (1892-1969), Ernst Keyssner and Eugen Dorrer and patented by I.G. Farben in the USA in 1937. [4] [1] PVK was the first polymer whose photoconductivity was known.
Many semicarbazones are crystalline solids, useful for the identification of the parent aldehydes/ketones by melting point analysis. [ 1 ] A thiosemicarbazone is an analog of a semicarbazone which contains a sulfur atom in place of the oxygen atom.