Search results
Results from the WOW.Com Content Network
where is the number of theoretical plates (also called the "plate count"), H is the total bed height and HETP is the height equivalent to a theoretical plate. The material in packed beds can either be random dumped packing (1-3" wide) such as Raschig rings or structured sheet metal.
For a packed column, the cross-sectional area of the column exit flow path is usually taken as 0.6 times the cross-sectional area of the column. Alternatively, the linear velocity can be taken as the ratio of the column length to the dead time. If the mobile phase is a gas, then the pressure correction must be applied.
In 1943 Dr Olaf George Dixon of ICI applied for a patent of a new product for column distillation. [1] He used stainless steel mesh instead of sheet steel in the Lessing ring in order to improve the pressure drop of the packed column (in fact, they were called "wire gauze Lessing rings" in a 1949 publication [2]).
The column bed can be filled with randomly dumped packing material (creating a random packed bed) or with structured packing sections, which are arranged in a way that force fluids to take complicated paths through the bed (creating a structured packed bed). In the column, liquids tend to wet the surface of the packing material and the vapors ...
Random column packing is the practice of packing a distillation column with randomly fitting filtration material in order to optimize surface area over which reactants can interact while minimizing the complexity of construction of such columns. Random column packing is an alternative to structured column packing.
Proper column packing is important for maximum resolution: An over-packed column can collapse the pores in the beads, resulting in a loss of resolution. An under-packed column can reduce the relative surface area of the stationary phase accessible to smaller species, resulting in those species spending less time trapped in pores.
A Raschig ring is a piece of tube, approximately equal in length and diameter, used in large numbers as a packed bed within columns for distillations and other chemical engineering processes. They are usually ceramic, metal, or glass and provide a large surface area within the volume of the column for interaction between liquid and gas vapours.
An a × b rectangle can be packed with 1 × n strips if and only if n divides a or n divides b. [15] [16] de Bruijn's theorem: A box can be packed with a harmonic brick a × a b × a b c if the box has dimensions a p × a b q × a b c r for some natural numbers p, q, r (i.e., the box is a multiple of the brick.) [15]