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Samples may become contaminated by titanium if they have line-of-sight to the pump. Also, titanium is a very hard material, so titanium film which builds up on the inside of the chamber may form flakes which fall into mechanical components (typically turbomolecular pumps and valves) and damage them. Many chambers containing TSPs also have an ...
Ion pumps; Titanium sublimation pumps; Non-evaporable getter (NEG) pumps; Cryopumps; Diffusion pumps, especially when used with a cryogenic trap designed to minimize backstreaming of pump oil into the systems. Turbo pumps and diffusion pumps rely on supersonic attack upon system molecules by the blades and high speed vapor stream, respectively.
A sublimatory [1] [2] or sublimation apparatus is equipment, commonly laboratory glassware, for purification of compounds by selective sublimation. In principle, the operation resembles purification by distillation , except that the products do not pass through a liquid phase .
Getter pump or sorption pump In laboratory vacuum systems, the bulk NEG getter is often held in a separate vessel with its own heater, attached to the vacuum system by a valve, so that it can be replaced or renewed when saturated. [8] Ion getter pump Uses a high voltage electrode to ionize the gas molecules and drive them into the getter surface.
Reciprocating pumps include plunger, diaphragm, and piston pumps. The high-density solids pumps which can be used in the widest range of situations are piston (or reciprocating) pumps. They can be realized as single-cylinder or two-cylinder pumps. In the latter case, power is transferred to the material via delivery pistons working in push-pull ...
The processing of titanium metal occurs in four major steps: reduction of titanium ore into "sponge", a porous form; melting of sponge, or sponge plus a master alloy to form an ingot; primary fabrication, where an ingot is converted into general mill products such as billet, bar, plate, sheet, strip, and tube; and secondary fabrication of ...
A noble diode pump is a type of ion pump used in high-vacuum applications that employs both a chemically reactive cathode, such as titanium, and an additional cathode composed of tantalum. The tantalum cathode serves as a high-inertia crystal lattice structure for the reflection and burial of neutrals, increasing pumping effectiveness of inert ...
The traditional method involves treatment of titanium tetrachloride with excess hydrogen fluoride: [3] TiCl 4 + 4 HF → TiF 4 + 4 HCl. Purification is by sublimation, which involves reversible cracking of the polymeric structure. [4] X-ray crystallography reveals that the Ti centres are octahedral, but conjoined in an unusual columnar ...