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[4] Compared with destructive techniques, e.g. three-dimensional electron backscatter diffraction (3D EBSD), [5] with which the sample is serially sectioned and imaged, 3DXRD and similar X-ray nondestructive techniques have the following advantages: They require less sample preparation, thus limiting the introduction of new structures in the ...
Typically the curves are staggered both across the screen and vertically, with "nearer" curves masking the ones behind. The result is a series of "mountain" shapes that appear to be side by side. The waterfall plot is often used to show how two-dimensional information changes over time or some other variable such as rotational speed.
Most often the filtered back projection reconstruction algorithm [10] is employed to reconstruct the XRD-CT images. The outcome is an image in which every pixel, or more accurately voxel, equates to a local diffraction pattern. The reconstructed data can also be seen as a stack of 2D square images, where each image corresponds to an X-ray ...
The results were presented to the Bavarian Academy of Sciences and Humanities in June 1912 as "Interferenz-Erscheinungen bei Röntgenstrahlen" (Interference phenomena in X-rays). [ 20 ] [ 21 ] Von Laue developed a law that connects the scattering angles and the size and orientation of the unit-cell spacings in the crystal, for which he was ...
[2] [4] Since different sample orientations provide different projections of the reciprocal lattice, they provide an opportunity to reconstruct the three-dimensional information lost in individual projections. A series of diffractograms varying in tilt can be acquired and processed with diffraction tomography analysis in order to reconstruct an ...
This is useful if the sample is too thick for X-rays to transmit through it. The diffracting planes in the crystal are determined by knowing that the normal to the diffracting plane bisects the angle between the incident beam and the diffracted beam. A Greninger chart can be used [30] to interpret the back reflection Laue photograph.
Small-angle X-ray scattering (SAXS) is a small-angle scattering technique by which nanoscale density differences in a sample can be quantified. This means that it can determine nanoparticle size distributions, resolve the size and shape of (monodisperse) macromolecules, determine pore sizes, characteristic distances of partially ordered materials, and much more. [1]
In X-ray crystallography, wide-angle X-ray scattering (WAXS) or wide-angle X-ray diffraction (WAXD) is the analysis of Bragg peaks scattered to wide angles, which (by Bragg's law) are caused by sub-nanometer-sized structures. [1]